• 专利标题:   Method for preparing graphene/zinc oxide nano composite material that is utilized in gas sensor for detecting ethanolamine, involves dissolving graphene oxide and zinc nitrate, followed by transferring resultant solution to reaction kettle.
  • 专利号:   CN104007236-A
  • 发明人:   DU J, ZHAO R, YAO H
  • 专利权人:   UNIV TAIYUAN TECHNOLOGY
  • 国际专利分类:   B82Y030/00, G01N033/00
  • 专利详细信息:   CN104007236-A 27 Aug 2014 G01N-033/00 201477 Chinese
  • 申请详细信息:   CN104007236-A CN10221606 26 May 2014
  • 优先权号:   CN10221606

▎ 摘  要

NOVELTY - A graphene/zinc oxide nano composite material preparing method involves dissolving 0.0005-0.001 pts. wt. graphene oxide and 2.5-3 pts. wt. zinc nitrate in water ultrasonically by adding 0.05-0.06 pts. wt. hexadecyl alkyl trimethyl ammonium bromide for 30-45 minutes to obtain a resultant solution. The resultant solution is added with hydrazine hydrate ultrasonically for 30-45 minutes. The obtained solution is transferred in a reaction kettle. The kettle is cooled at room temperature to obtain reactant. The reactant is centrifuged, washed and dried to obtain a finished product. USE - Method for preparing graphene/zinc oxide nano composite material that is utilized in gas sensor for detecting ethanolamine (claimed). DETAILED DESCRIPTION - A graphene/zinc oxide nano composite material preparing method involves dissolving 0.0005-0.001 pts. wt. graphene oxide and 2.5-3 pts. wt. zinc nitrate in water ultrasonically by adding 0.05-0.06 pts. wt. hexadecyl alkyl trimethyl ammonium bromide for 30-45 minutes to obtain a resultant solution. The resultant solution is added with hydrazine hydrate ultrasonically for 30-45 minutes according to zinc nitrate and water at a mass volume ratio of 3.8 (w/v)%, and zinc nitrate and hydrazine hydrate mass volume ratio of 50(w/v)%. The obtained solution is transferred in a reaction kettle at 150-160 degrees C for 12-14 hours. The kettle is cooled at room temperature to obtain reactant. The reactant is centrifuged, washed and dried to obtain a finished product.