• 专利标题:   Making dispersion of graphene particles or sheets comprises providing block of solid material made of graphite, scraping material surface of substrate and dipping substrate in liquid medium and subjecting liquid medium to ultrasound.
  • 专利号:   FR2952049-A1, FR2952049-B1
  • 发明人:   JANOWSKA I, BEGIN D, CHIZARI K, ERSEN O, BERNHARDT P, ROMERO T, LEDOUX M, PHAM H C
  • 专利权人:   CENT NAT RECH SCI, UNIV STRASBOURG
  • 国际专利分类:   B82B003/00, C01B031/02
  • 专利详细信息:   FR2952049-A1 06 May 2011 C01B-031/02 201132 Pages: 34 French
  • 申请详细信息:   FR2952049-A1 FR005252 03 Nov 2009
  • 优先权号:   FR005252

▎ 摘  要

NOVELTY - Preparing a dispersion of graphene particles or sheets in a liquid medium (6), comprises: (a) providing a bar or block (5) of solid material made of graphite; (b) scraping the material surface (2) of a substrate to create a trace of scraping of the material on the surface of the substrate; and (c) dipping the substrate in a liquid medium and subjecting the liquid medium to ultrasound, where the steps (b) and (c) are performed at least in part, simultaneously. USE - The dispersion of graphene particles or sheets is useful in the manufacture of polymer composites, composite materials, final composite and electronic circuits. ADVANTAGE - The process: provides a dispersion of graphene particles or sheets with high yield; and is inexpensive and suitable for industrial scale preparation. The process avoids external heating or addition of toxic chemicals. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a device for carrying out the process comprising an arm (3) capable of holding the bar or block (5) in bulk material, a substrate provided with a surface (2) contacting the bar or block in bulk material, a means of shifting to generate a relative displacement between the solid material and the substrate, a means of regulating and/or controlling the force of pressure for regulating, consistently maintaining and/or measuring the pressure between the solid material and surface of the substrate during the relative movement, a liquid reservoir for immersing at least partially the surface in a liquid medium (6), an ultrasound generator (7) for subjecting the liquid to the ultrasound effect. DESCRIPTION OF DRAWING(S) - The figure shows a schematic representation of a device for preparing dispersion of graphene particles or sheets. Surface (2) Arm (3) Bar or Block (5) Liquid phase (6) Ultrasound generator. (7)