• 专利标题:   Nickel-iron hydroxide/reduced graphene oxide electrochemical oxygen evolution catalyst comprises nickel foam as a carrier, iron hydroxide or nickel hydroxide as active components and reduced graphene oxide as a conductive material.
  • 专利号:   CN108707923-A
  • 发明人:   SHAO D, LI P, ZHOU Y
  • 专利权人:   UNIV EAST CHINA SCI TECHNOLOGY
  • 国际专利分类:   C25B011/03, C25B011/06, C25B001/04, C23C018/12
  • 专利详细信息:   CN108707923-A 26 Oct 2018 C25B-011/03 201879 Pages: 6 Chinese
  • 申请详细信息:   CN108707923-A CN10592304 11 Jun 2018
  • 优先权号:   CN10592304

▎ 摘  要

NOVELTY - Nickel-iron hydroxide/reduced graphene oxide electrochemical oxygen evolution catalyst comprises nickel foam as a carrier, iron hydroxide and/or nickel hydroxide as active components and reduced graphene oxide as a conductive material. USE - Used as nickel-iron hydroxide/reduced graphene oxide electrochemical oxygen evolution catalyst. ADVANTAGE - The catalyst has good catalytic activity and high stability. The method is simple and controllable and is suitable for industrial production. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing the catalyst, comprising (a) ultrasonic cleaning of foamed nickel and drying; (b) dissolving nickel salt and urea in deionized water and stirring at room temperature to obtain a homogeneous mixture; (c) adding graphene oxide to the mixture in step (b), subjecting to ultrasonic treatment in an ultrasonic bath to obtain a uniformly dispersed mixture; (d) transferring foamed nickel and mixture into a hydrothermal kettle and reacting at 120-200 degrees C for 12-24 hours; (e) washing foamed nickel with ethanol and deionized water and drying; and (f) immersing foamed nickel in 5-30 mmol/l iron salt for 0-48 hours and washing with ethanol and deionized water and drying.