• 专利标题:   Preparing graphene oxide or graphite oxide comprises e.g. adding concentrated sulfuric acid, graphite, potassium permanganate and water into reaction kettle, stirring and controlling reaction temperature and reaction time and purifying.
  • 专利号:   CN112645317-A, CN216141264-U
  • 发明人:   WANG B, YIN S, ZHANG J, GE M, TANG R, QU Y
  • 专利权人:   NANTONG SIXTH ELEMENT MATERIALS TECHNOLOGY CO LTD, SIXTH ELEMENT CHANGZHOU MATERIALS TECHNO, NANTONG SIXTH ELEMENT MATERIALS TECHNOLO
  • 国际专利分类:   C01B032/198, C01B032/23
  • 专利详细信息:   CN112645317-A 13 Apr 2021 C01B-032/198 202143 Pages: 19 Chinese
  • 申请详细信息:   CN112645317-A CN11617350 30 Dec 2020
  • 优先权号:   CN11617350, CN23297285

▎ 摘  要

NOVELTY - Preparing graphene oxide or graphite oxide comprises (i) adding concentrated sulfuric acid, graphite, potassium permanganate and water into the reaction kettle, stirring and controlling the reaction temperature and reaction time to obtain the graphene oxide or graphite oxide slurry, the salt in the graphene oxide or graphite oxide slurry to form a supersaturated state, (ii) purifying the graphene oxide or oxidized graphite slurry, separating and removing salt particles, (iii) performing purification treatment to the material to obtain the cake material with high solid content, dry material or slurry state material, (iv) mixing and dispersing the cake material, dry material or slurry state material with water to form the material with low solid content of slurry or solution state, (v) re-purifying the slurry or solution state to obtain the cake material with high solid content, dry material or slurry state material, and (vi) repeatedly executing the step (iv) and (v) for many times. USE - The method is useful for preparing graphene oxide or graphite oxide. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for device for producing graphene oxide or graphite oxide.