• 专利标题:   Preparation of high-strength graphene fibers used for flexible energy storage device by adding Hummers graphite oxide in distilled water, sonicating, adding sodium polyacrylate, pushing into coagulation bath, hydroiodic reducing and drying.
  • 专利号:   CN104894692-A, CN104894692-B
  • 发明人:   HOU C, LI Y, WANG H, ZHANG Q, SHI Q
  • 专利权人:   UNIV DONGHUA
  • 国际专利分类:   D01F011/12, D01F009/12
  • 专利详细信息:   CN104894692-A 09 Sep 2015 D01F-009/12 201601 Pages: 9 Chinese
  • 申请详细信息:   CN104894692-A CN10299073 03 Jun 2015
  • 优先权号:   CN10299073

▎ 摘  要

NOVELTY - Preparation of high-strength graphene fibers comprises adding Hummers graphite oxide in distilled water, sonicating to get graphite oxide dispersion, adding sodium polyacrylate, magnetic stirring to obtain uniform graphene oxide/sodium polyacrylate gel dope; pushing using syringe into coagulation bath, drying for 0.5-1 hour to get graphene oxide fiber; and carrying out hydroiodic reduction for 0.5-1 hour, cleaning and drying. The ratio of sodium polyacrylate and graphite oxide dispersion is 5-20 mg:1 ml. USE - Method for preparing high-strength graphene fibers (claimed) used for flexible energy storage device. ADVANTAGE - The method is simple, inexpensive, and easy to be industrialized. The strong fiber has high quality, large intensity, stable performance and good flexibility.