• 专利标题:   Preparing highly fluorescent boron-nitrogen co-doped graphene quantum dots by one-pot hydrothermal method comprises e.g. dissolving citric acid, urea and borax in ultrapure water, carrying out hydrothermal reaction, dialyzing and drying.
  • 专利号:   CN110922967-A
  • 发明人:   MO Z, LIU Z, GUO R, LIU N, NIU X, YANG X
  • 专利权人:   UNIV NORTHWEST NORMAL
  • 国际专利分类:   B82Y020/00, B82Y030/00, C01B032/184, C09K011/65
  • 专利详细信息:   CN110922967-A 27 Mar 2020 C09K-011/65 202035 Pages: 8 Chinese
  • 申请详细信息:   CN110922967-A CN11356626 25 Dec 2019
  • 优先权号:   CN11356626

▎ 摘  要

NOVELTY - Preparing highly fluorescent boron-nitrogen co-doped graphene quantum dots by one-pot hydrothermal method comprises taking citric acid as carbon source, urea as nitrogen source and borax as boron source, then completely dissolving in ultrapure water, placing in high-pressure kettle, and carrying out hydrothermal reaction at 180-200 degrees C for 1.5-2 hours, and cooling to room temperature to obtain aqueous solution of boron-nitrogen co-doped graphene quantum dots in brownish black color, then dialyzing aqueous solution of boron-nitrogen co-doped graphene quantum dots in 3000 Da dialysis bag for 1-2 days, concentrating dialyzed aqueous solution of boron-nitrogen co-doped graphene quantum dots by rotary evaporation, and drying to obtain brown-green high-fluorescent boron-nitrogen co-doped graphene quantum dot powder. USE - The highly fluorescent boron-nitrogen co-doped graphene quantum dots is useful in fluorescence sensors, biological imaging, optoelectronic devices and other aspects. ADVANTAGE - The quantum dots have high crystallinity, strong water solubility, narrow lateral size distribution, low biological toxicity, high biocompatibility and excellent luminescence behavior. The method has simple process, strong controllability and high quantum yield.