• 专利标题:   Preparing graphene oxide/poly dopamine composite airgel comprises e.g. dissolving dopamine powder, adding graphene oxide, mixing, stirring, dropping tris buffer, carrying out polymerization reaction of dopamine freezing and drying.
  • 专利号:   CN105254916-A
  • 发明人:   DAI J, HUANG T, WANG Y, YANG J, ZHANG N
  • 专利权人:   UNIV SOUTHWEST JIAOTONG
  • 国际专利分类:   B01J020/26, B01J020/28, B01J020/30, C08G073/02, C08J003/075, C08J009/28, C08K003/04, C08K009/02, C08L079/02
  • 专利详细信息:   CN105254916-A 20 Jan 2016 C08J-009/28 201624 Pages: 8 English
  • 申请详细信息:   CN105254916-A CN10642379 30 Sep 2015
  • 优先权号:   CN10642379

▎ 摘  要

NOVELTY - Preparing graphene oxide/poly dopamine composite airgel comprises (i) dissolving dopamine powder in distilled water, adding graphene oxide, mixing to obtain a graphene oxide/dopamine mixed solution, (ii) stirring and dropping tris buffer, continuing stirring, allowing to stand, carrying out polymerization reaction of dopamine to obtain graphene oxide/poly dopamine composite hydrogel, (iii) placing the graphene oxide/poly dopamine composite hydrogel under -20 to -10 degrees C for 24-30 hours, freezing and drying. USE - The method is useful for preparing graphene oxide/poly dopamine composite airgel (claimed). ADVANTAGE - The gel has high porosity and excellent adsorption property. DETAILED DESCRIPTION - Preparing graphene oxide/poly dopamine composite airgel comprises (i) dissolving 0.15-0.7 g dopamine powder in 10-18 ml distilled water, adding 50-60 ml of 5-6 mg/ml graphene oxide, mixing to obtain a aqueous solution, stirring for 30-40 minutes to obtain graphene oxide/dopamine mixed solution, (ii) stirring and dropping 3-9 ml of 0.1-0.12 mol/l tris buffer, continuing stirring for 2-2.5 hours, allowing to stand, carrying out polymerization reaction of dopamine to obtain graphene oxide/poly dopamine composite hydrogel, (iii) placing the graphene oxide/poly dopamine composite hydrogel under -20 to -10 degrees C for 24-30 hours, freezing and drying.