• 专利标题:   Preparation of nitrogen-doped graphene adsorbent from aerobic granular sludge used for removal of anionic dye in water by drying sludge, grinding, sieving, carbonizing inn furnace, adding to hydrochloric acid, centrifuging and washing.
  • 专利号:   CN106902758-A
  • 发明人:   LI N, WEI D, DU B, YAN T, HU L, WANG X
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   B01J020/24, B01J020/28, C02F001/28, C02F101/30, C02F103/30
  • 专利详细信息:   CN106902758-A 30 Jun 2017 B01J-020/24 201754 Pages: 7 Chinese
  • 申请详细信息:   CN106902758-A CN10194004 28 Mar 2017
  • 优先权号:   CN10194004

▎ 摘  要

NOVELTY - Preparation of nitrogen-doped graphene adsorbent from aerobic granular sludge comprises drying aerobic granular sludge from culture laboratory sequencing batch reactor at 100-110 degrees C, grinding, sieving to 100-150 mesh, putting in tubular furnace, carbonizing at 800-900 degrees C for 5-6 hours at heating rate of 12-15 degrees C/minute under nitrogen protective gas, cooling to room temperature to obtain black powder, taking out, adding into 4-8 mol/L hydrochloric acid, removing impurities, centrifuging, washing with deionized water until neutral, and drying at 100-110 degrees C to constant weight. USE - Method for preparing nitrogen-doped graphene adsorbent from aerobic granular sludge used for removal of anionic dye in water (claimed). ADVANTAGE - The method is simple and easy, has low cost, high absorption capacity and no secondary pollution, and can be used repeatedly. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for removal of anionic dye in water comprising adding 20-40 mL of 10-30 mg/L anionic dye solution to 50-mL conical flask, adding 20-40 mg nitrogen-doped graphene adsorbent, oscillating at 20-40 degrees C for 2-4 hours, taking out mixed solution, centrifuging, taking supernatant, measuring absorbance by spectrophotometer, drawing concentration-absorbance working curve of anionic dye and calculating removal rate.