• 专利标题:   Preparing nitrogen-phosphorus co-doped graphene carbon material comprises e.g. mixing aqueous graphene oxide solution and dopamine aqueous solution, then adding 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide solution and stirring.
  • 专利号:   CN108584905-A
  • 发明人:   PENG C, CENG T, YU Y
  • 专利权人:   UNIV HUNAN AGRIC
  • 国际专利分类:   C01B032/05, C01B032/182
  • 专利详细信息:   CN108584905-A 28 Sep 2018 C01B-032/05 201871 Pages: 8 Chinese
  • 申请详细信息:   CN108584905-A CN10429284 25 Apr 2018
  • 优先权号:   CN10429284

▎ 摘  要

NOVELTY - Preparing nitrogen-phosphorus co-doped graphene carbon material, comprises (i) mixing aqueous graphene oxide solution and dopamine aqueous solution under stirring, and adding 10-20 ml alkaline phosphate buffered saline solution, and stirring at room temperature for 20-24 hours, (ii) adding 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide solution to the mixed solution after step (i), and stirring at room temperature for 12-14 hours to obtain black solution and then subjecting black solution to solid-liquid separation to obtain a solid product, then washing the solid product with water 2-3 times, alcohol washing for 2-3 times and drying to obtain black solid, and (iii) subjecting black solid obtained in the step (ii) to a high temperature treatment at 700-900 degrees C for 3-6 hours in a tube furnace under inert gas protection to obtain final product. USE - The nitrogen-phosphorus co-doped graphene carbon material is useful in biosensor (claimed). ADVANTAGE - The method is simple and easy to operate. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for nitrogen-phosphorus co-doped graphene carbon material is obtained by above method.