• 专利标题:   Spinel-type ferromagnet/graphene nanocomposite for detecting small molecules of hydrogen peroxide and glucose, comprises iron oxide magnetic nanoparticles with uniform particle size and graphene.
  • 专利号:   CN105513740-A
  • 发明人:   ZHAO X, ZHU Z
  • 专利权人:   UNIV SHANGHAI SECOND POLYTECHNIC
  • 国际专利分类:   H01F001/36
  • 专利详细信息:   CN105513740-A 20 Apr 2016 H01F-001/36 201652 Pages: 10 English
  • 申请详细信息:   CN105513740-A CN10884428 07 Dec 2015
  • 优先权号:   CN10884428

▎ 摘  要

NOVELTY - A spinel-type ferromagnet/graphene nanocomposite comprises iron oxide magnetic nanoparticles with uniform particle size and graphene. USE - Spinel-type ferromagnet/graphene nanocomposite is used for detecting small molecules of hydrogen peroxide and glucose (all claimed). ADVANTAGE - The nanocomposite is prepared economically by simple process. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of spinel-type ferromagnet/graphene nanocomposite. 0.03-0.3 g graphene oxide is added to reaction apparatus containing 20-200 mL diethylene glycol solvent and ultrasonically dispersing for 1-5 hours. Then, 0.12-1.2 g ferromagnetic divalent metal salt is added and stirred at 190-220 degrees C for 0.5-2 hours under inert gas protection. Then, 10-100 mg/mL sodium hydroxide/5-50 mL stock solution is added to the mixture, heated at 190-220 degrees C for 1-5 hours, centrifuged and washed, to obtain spinel-type ferromagnet/graphene nanocomposite. The ferromagnetic divalent metal salt is zinc salt, cobalt salt, nickel salt, manganese salt or copper salt.