• 专利标题:   Preparation of zinc sulfide-graphene nanocomposite involves sintering mercaptozinc complex, naturally cooling resultant material to room temperature, soaking resultant sintered component in acid solution, filtering and drying.
  • 专利号:   CN105347388-A, CN105347388-B
  • 发明人:   CHEN P, HAN B, PAN R, ZHANG K, ZHANG S
  • 专利权人:   NANJING INST TECHNOLOGY
  • 国际专利分类:   B82Y030/00, C01G009/08
  • 专利详细信息:   CN105347388-A 24 Feb 2016 C01G-009/08 201643 Pages: 8 Chinese
  • 申请详细信息:   CN105347388-A CN10663049 14 Oct 2015
  • 优先权号:   CN10663049

▎ 摘  要

NOVELTY - Preparation of zinc sulfide-graphene nanocomposite involves dissolving sulfur-containing ligand and zinc salt in deionized water or organic solvent, reacting, stirring, performing centrifugal washing with organic solvent and deionized water, collecting precipitate, drying the precipitate, obtaining mercaptozinc complex, sintering the mercaptozinc complex, introducing nitrogen into the vacuum sintering furnace, naturally cooling the resultant material to room temperature, soaking the resultant sintered component in an acid solution, filtering and drying. USE - Preparation of zinc sulfide-graphene nanocomposite (claimed). ADVANTAGE - The method provides zinc sulfide-graphene nanocomposite by simple process in a short period of time. DETAILED DESCRIPTION - Preparation of zinc sulfide-graphene nanocomposite involves dissolving sulfur-containing ligand and zinc salt in deionized water or organic solvent, reacting, stirring, carrying out centrifugal washing with organic solvent and deionized water, collecting precipitate, drying the precipitate in vacuum, obtaining mercaptozinc complex, sintering the mercaptozinc complex in a vacuum sintering furnace, introducing nitrogen into the vacuum sintering furnace, naturally cooling the resultant material to room temperature, soaking the resultant sintered component in an acid solution, filtering and drying.