• 专利标题:   Preparation of aqueous dispersion of graphene involves adding dispersion liquid formed of graphene powder and water, to vacuum ultrasound apparatus, processing and stabilizing resultant dispersion in stabilized electric field device.
  • 专利号:   CN106009787-A, CN106009787-B
  • 发明人:   CHEN C, LI X, KONG Q, XIE L, SU F, HE J
  • 专利权人:   INST COAL CHEM CHINESE ACAD SCI, INST COAL CHEM CHINESE ACAD SCI
  • 国际专利分类:   C09C001/46, C09C003/04, C09C003/06
  • 专利详细信息:   CN106009787-A 12 Oct 2016 C09C-001/46 201682 Pages: 15 Chinese
  • 申请详细信息:   CN106009787-A CN10330047 18 May 2016
  • 优先权号:   CN10330047

▎ 摘  要

NOVELTY - Preparation of aqueous dispersion of graphene involves mixing graphene powder and water, obtaining graphene pre-wetting fluid, transferring graphene pre-wetting liquid to primary dispersing apparatus, stirring, obtaining primary dispersion liquid, adding obtained primary dispersion to vacuum ultrasound apparatus, processing for 1-30 minutes, obtaining secondary dispersion liquid, placing obtained dispersion in stabilized electric field device, applying voltage of 50-1000 V, and stabilizing for 10-300 seconds. USE - Preparation of aqueous dispersion of graphene (claimed). ADVANTAGE - The method stably and economically provides aqueous dispersion of graphene having high dispersion degree, by simple method without affecting the environment. DETAILED DESCRIPTION - Preparation of aqueous dispersion of graphene involves mixing graphene powder and water in the mass ratio of 1:9-999, adding to stirring vessel, stirring using stirrer, adjusting the rotational speed of the agitator as 10-500 rpm, stirring for 10-30 minutes, obtaining graphene pre-wetting fluid, transferring the graphene pre-wetting liquid to primary dispersing apparatus, controlling rotational speed as 1000-10000 rpm, obtaining primary dispersion liquid, adding obtained primary dispersion to vacuum ultrasound apparatus in the vacuum pressure of -0.01 MPa to -0.1 MPa and ultrasonic power of 500-2000 W, processing for 1-30 minutes, obtaining secondary dispersion liquid, placing obtained dispersion in stabilized electric field device, applying voltage of 50-1000 V, and stabilizing for 10-300 seconds.