• 专利标题:   Continuously preparing high performance nano-carbon fiber, comprises e.g. mixing nanocarbon material with acid solution, injecting spinning solution into coagulation bath to solidify and carrying out heat treatment.
  • 专利号:   CN113913970-A
  • 发明人:   QU S, ZHU Q, LV W
  • 专利权人:   CHINESE ACAD SCI SUZHOU NANOTECH NANO
  • 国际专利分类:   D01D005/06, D01D005/14, D01F011/12, D01F011/14, D01F009/12
  • 专利详细信息:   CN113913970-A 11 Jan 2022 D01F-009/12 202238 Chinese
  • 申请详细信息:   CN113913970-A CN11431466 29 Nov 2021
  • 优先权号:   CN11431466

▎ 摘  要

NOVELTY - Continuously preparing high performance nano-carbon fiber, comprises (i) mixing the nanocarbon material with acid solution to obtain spinning solution; (ii) injecting the spinning solution into the coagulation bath to solidify, and drafting; (iii) carrying out heat treatment to obtain the nanometre carbon fiber after the drafting, where the coagulation bath redrafting operation is repeated for at least 2 times. The nanocarbon material comprises carbon nanotube, graphene, graphene oxide or fullerene and the acid solution comprises chlorosulfonic acid, fuming sulfuric acid, trifluoromethanesulfonic acid or fluorine sulfuric acid. USE - The method is useful for continuously preparing high performance nano-carbon fiber. ADVANTAGE - The method adopts multi-stage gradient coagulation bath to form; and applies a certain drafting in the forming process, which effectively improves the performance of the nanometre carbon fiber. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for nano-carbon fiber.