• 专利标题:   Boron-nitrogen-doped three-dimensional graphene block preparation used in lithium-sulfur battery, involves mixing biomass material, boron oxide, nitrogen precursor, metal catalyst precursor and solvent with stirring.
  • 专利号:   CN107342406-A, CN107342406-B
  • 发明人:   HUANG F, XU J
  • 专利权人:   SHANGHAI INST CERAMICS CHINESE ACAD SCI
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/587, H01M004/62
  • 专利详细信息:   CN107342406-A 10 Nov 2017 H01M-004/36 201783 Pages: 13 Chinese
  • 申请详细信息:   CN107342406-A CN10480512 22 Jun 2017
  • 优先权号:   CN10480512

▎ 摘  要

NOVELTY - Boron-nitrogen-doped three-dimensional graphene block preparation involves mixing biomass material, boron oxide, nitrogen precursor, metal catalyst precursor and solvent with stirring at 80-100 degrees C to obtain precursor solution. The biomass material, boron oxide precursor, nitrogen, catalyst precursor and metal mass in a ratio of 1:0.5-2:0-2:0.5-2. The solvent is water or a mixed solution of water and ethanol. The resulting precursor solution is cooled to form a three-dimensional gel. USE - Method for preparing boron-nitrogen-doped three-dimensional graphene block used in lithium-sulfur battery (claimed). ADVANTAGE - The method prepares the boron-nitrogen-doped three-dimensional graphene block in a simple and cost-effective manner. DETAILED DESCRIPTION - Boron-nitrogen-doped three-dimensional graphene block preparation involves mixing biomass material, boron oxide, nitrogen precursor, metal catalyst precursor and solvent with stirring at 80-100 degrees C to obtain precursor solution. The biomass material, boron oxide precursor, nitrogen, catalyst precursor and metal mass in a ratio of 1:0.5-2:0-2:0.5-2. The solvent is water or a mixed solution of water and ethanol. The resulting precursor solution is cooled to form a three-dimensional gel. The resulting three-dimensional gel is freeze-dried to obtain boron and nitrogen co-doped three-dimensional graphene block. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic view of the Brunauer-Emmett-Teller test pattern of the boron-nitrogen-doped three-dimensional graphene block. (Drawing includes non-English language text).