• 专利标题:   Preparing multifunctional bio-based degradable polylactic acid resin used for preparing multifunctional bio-based degradable polylactic acid fiber, involves performing chelation of graphene oxide and tin ions in tin-containing compound.
  • 专利号:   CN111187496-A
  • 发明人:   ZHOU J, ZHU M, YU S, XIANG H, DI G, HOU K, ZHOU Z
  • 专利权人:   UNIV DONGHUA
  • 国际专利分类:   C08G063/08, C08G063/78, C08K003/04, C08K003/22, C08K005/5313, C08K009/12, C08L067/04, D01F001/07, D01F001/09, D01F008/14
  • 专利详细信息:   CN111187496-A 22 May 2020 C08L-067/04 202049 Pages: 8 Chinese
  • 申请详细信息:   CN111187496-A CN10087842 12 Feb 2020
  • 优先权号:   CN10087842

▎ 摘  要

NOVELTY - Preparing multifunctional bio-based degradable polylactic acid resin involves performing chelation of graphene oxide with a carboxylation ratio of 10-30 wt.% and tin ions in a tin-containing compound to obtain first material. The obtained first material material is undergoes heat treatment to obtain second material. The second material and lactide are reacted under vacuum conditions of 200-240 degrees C for 6-15 hours to obtain reduced graphene oxide (RGO)-polylactic acid. The rGO-polylactic acid with polylactic acid and metal salts of alkylphosphinic acid are undergoes melt blending to prepare the multifunctional bio-based degradable polylactic acid resin. USE - Method for preparing multifunctional bio-based degradable polylactic acid resin used for preparing multifunctional bio-based degradable polylactic acid fiber by a melt spinning method (claimed). ADVANTAGE - The method enables to prepare multifunctional bio-based degradable polylactic acid resin which can effectively improve its dispersibility and facilitate the large-scale production of polylactic acid fibers.