• 专利标题:   Preparing graphene-graphene nano ribbon sponge comprises e.g. determining concentration of graphene oxide and graphene oxide nano ribbon solutions by gravity method, extracting corresponding volume of solution into mold, and stirring.
  • 专利号:   CN110872112-A
  • 发明人:   JI Y
  • 专利权人:   JI Y
  • 国际专利分类:   C01B032/184, H01G011/32
  • 专利详细信息:   CN110872112-A 10 Mar 2020 C01B-032/184 202028 Pages: 4 Chinese
  • 申请详细信息:   CN110872112-A CN11019241 03 Sep 2018
  • 优先权号:   CN11019241

▎ 摘  要

NOVELTY - Preparing graphene-graphene nano ribbon sponge comprises (1) determining concentration of graphene oxide (GO) and graphene oxide nano ribbon (GONR) solutions by gravity method, in mg/ml, (2) according to the mass ratio of GO to GONR is 1:1, extracting corresponding volume of solution into the mold, stirring and mixing, (3) mixing GO-GONR solution in the cold well of the freeze dryer for about 24 hours, and evacuating to start freeze-drying to ensure that the sample is completely dry, the freeze-drying time needs at least 48 hours, (4) taking out the freeze-dried sample at this time, it is the GO-GONR ribbon that has not been reducing, i.e., graphene oxide-graphene oxide nano ribbon composite sponge, (5) reducing in 90 degrees C hydrazine hydrate for 24 hours, cooling, taking out, placing into a vacuum drying box at 100 degrees C for 24 hours for removing residual hydrazine hydrate, and cooling to room temperature to obtain graphene-graphene nano ribbon sponge. USE - The method is useful for preparing graphene-graphene nano ribbon sponge. ADVANTAGE - The method: has simple operation.