• 专利标题:   Preparing graphene by condensing graphene oxide and isooctanol as raw materials and p-toluenesulfonic acid as catalyst, refluxing, charging reaction base with ester base oil, cooling, dehydrating, distilling, centrifuging and filtering.
  • 专利号:   CN110407199-A
  • 发明人:   CAI G, MA Y, CHEN B, WANG W
  • 专利权人:   CHONGQING CHEM IND VOCATIONAL COLLEGE
  • 国际专利分类:   C01B032/194, C01B032/198, C10M141/02, C10M159/12, C10N030/06
  • 专利详细信息:   CN110407199-A 05 Nov 2019 C01B-032/194 201990 Pages: 6 Chinese
  • 申请详细信息:   CN110407199-A CN10766904 20 Aug 2019
  • 优先权号:   CN10766904

▎ 摘  要

NOVELTY - Method for preparing graphene, involves (a) taking graphene oxide and isooctanol as a raw materials and p-toluenesulfonic acid as a catalyst, condensing, refluxing at 183-186 degrees C for 8 hours, removing the water formed by the reaction using a water separator during the reaction, subsequently charging the reaction base with an ester base oil, stirring, and cooling to 90-100 degrees C, (b) cooling the reaction mixture to 90-100 degrees C until a pH value reaches 6.8-7.2, controlling vacuum pressure 1.01-0.70 kPa, dehydrating at 80-100 degrees C for 2-3 hours under reduced pressure, distilling at 150-170 degrees C for 2-4 hours under reduced pressure, centrifuging and filtering to obtain the product. USE - The method is useful for preparing graphene. ADVANTAGE - The prepared graphene exhibits excellent antiwear performance.