• 专利标题:   Preparing graphene pyrrole aerogel used in seawater desalination, involves preparing graphene oxide, adding reducing agent in graphene oxide dispersion liquid, stirring solution, placing in oven, and obtaining reduced graphene oxide hydrogel by hydrothermal reaction.
  • 专利号:   CN113926397-A, CN113926397-B
  • 发明人:   XU F, CAO Y
  • 专利权人:   UNIV XIAMEN
  • 国际专利分类:   B01J013/00, C01B032/192, C01B032/198, C02F001/14, C02F103/08
  • 专利详细信息:   CN113926397-A 14 Jan 2022 B01J-013/00 202261 Chinese
  • 申请详细信息:   CN113926397-A CN10674916 14 Jul 2020
  • 优先权号:   CN10674916

▎ 摘  要

NOVELTY - Preparing graphene pyrrole aerogel involves preparing graphene oxide, and adjusting graphene oxide to 5-50 mg/ml, adding reducing agent in the graphene oxide dispersion liquid, and the volume ratio of the two is 1-10:1-10. The solution is stirred, placed in an oven at 150-200degrees Celsius, and prepared reduced graphene oxide (RGO) hydrogel by hydrothermal reaction for 1-3 hours. The RGO hydrogel is taken out, washed with water until neutral, and then freeze-dried to form RGO aerogel. The 0.1-5 vol/vol.% pyrrole aqueous solution and 0.5-5 molar ammonium persulfate hydrochloride solution are configured. The RGO aerogel is immersed in the pyrrole aqueous solution until it is completely saturated, and saturated RGO is dried, then slowly immersed in ammonium persulfate hydrochloride solution, and polymerized at 1-5degrees Celsius for 5-10 hours. The samples are washed with deionized water and dried to obtain graphene-pyrrole aerogels. USE - Method for preparing graphene pyrrole aerogel used in seawater desalination (claimed). ADVANTAGE - The method utilizes clean and sustainable energy solar energy combined with joule heat testing unit to carry out seawater desalination tests alternately and continuously, and is a novel seawater desalination method with lower energy consumption and high efficiency. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: 1. a method for evaporating seawater desalination based on graphene-based aerogel interface film, which involves preparing graphene pyrrole aerogel, infiltrating and suspending the prepared graphene-based aerogel on the surface of seawater, and then under the irradiation of sunlight, heating the graphene-based aerogel realizes interface photothermal conversion through local heating, and desalinating seawater, and/or fixing the graphene-based aerogel that the hydrophobic treatment has been treated on the device of seawater desalination, and achieving the desalination of seawater with low energy consumption by using its own way of generating joule heat; and 2. graphene pyrrole aerogel.