• 专利标题:   Preparing graphene oxide-silver nanomaterial having high antibacterial properties involves reacting graphite, sodium nitrite, potassium permanganate and concentrated sulfuric acid, warming and adding deionized water.
  • 专利号:   CN107915221-A
  • 发明人:   SI R, PAN Z, LIU C
  • 专利权人:   TIANJIN BAOXINGWEI TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/198, B22F009/24, B22F001/00, B82Y040/00
  • 专利详细信息:   CN107915221-A 17 Apr 2018 C01B-032/198 201837 Pages: 5 Chinese
  • 申请详细信息:   CN107915221-A CN11327772 13 Dec 2017
  • 优先权号:   CN11327772

▎ 摘  要

NOVELTY - Preparing graphene oxide-silver nanomaterial having high antibacterial properties involves reacting 50 mg graphite, 0.5 g sodium nitrite, 3 g potassium permanganate and 23 ml concentrated sulfuric acid at 2-5 degrees C for 60-80 minutes, warming to 35-38 degrees C for 35-45 minutes followed by the addition of 60-80 ml deionized water, heating to 80-90 degrees C followed by the addition of hydrogen peroxide, centrifuging, washing and drying to obtain graphene oxide. USE - Method for preparing graphene oxide-silver nanomaterial having high antibacterial properties. DETAILED DESCRIPTION - Preparing graphene oxide-silver nanomaterial having high antibacterial properties involves reacting 50 mg graphite, 0.5 g sodium nitrite, 3 g potassium permanganate and 23 ml concentrated sulfuric acid at 2-5 degrees C for 60-80 minutes, warming to 35-38 degrees C for 35-45 minutes followed by the addition of 60-80 ml deionized water, heating to 80-90 degrees C followed by the addition of hydrogen peroxide, centrifuging, washing and drying to obtain graphene oxide. The preparation of graphene oxide-nanometer silver involves dissolving 3 mg of silver nitrate in 60 mL deionized water followed by the addition of 3 mg of oxidized stone enamel powder in 30 mL deionized water. The silver nitrate solution and graphene oxide solution are mixed using ultrasound for 20-30 minutes, heated to 95-105 degrees C, added sodium citrate with stirring for 20-30 minutes and allowed to precipitate for 6-10 hours. The precipitate is filtered under suction, washed and dried to obtain graphene oxide-silver nanomaterial having high antibacterial properties.