• 专利标题:   Preparing graphene mother liquor comprises e.g. dispersing graphene in aqueous solution of sodium polyphosphate, sonicating, mixing graphene-bentonite complex and organic solvent, adding surfactant, and dispersing.
  • 专利号:   CN107057006-A
  • 发明人:   CHEN Q, WANG L, ZENG J
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD
  • 国际专利分类:   C08G008/10, C08K013/06, C08K003/04, C08K003/32, C08K009/12
  • 专利详细信息:   CN107057006-A 18 Aug 2017 C08G-008/10 201774 Pages: 7 Chinese
  • 申请详细信息:   CN107057006-A CN10379156 25 May 2017
  • 优先权号:   CN10379156

▎ 摘  要

NOVELTY - Preparing graphene mother liquor comprises e.g. (i) dispersing 30-50 pts. wt. graphene in aqueous solution of sodium polyphosphate, sonicating, then adding 40-60 pts. wt. acidified modified nano bentonite, taking graphene and nano-bentonite as carrier, stable, uniform load in nano-bentonite, filtering, washing and drying to obtain graphene-bentonite complex, and (ii) mixing graphene-bentonite complex and 100-200 pts. wt. organic solvent, then adding 20-30 pts. wt. phenol into mixed system, stirring, and then adding 1-3 pts. wt. surfactant, and dispersing by magnetic stirring. USE - The graphene mother liquor is useful in thermosetting phenolic resin (claimed). ADVANTAGE - The method is simple, has short reaction condition, low cost, and is suitable for industrial production. DETAILED DESCRIPTION - Preparing graphene mother liquor comprises (i) dispersing 30-50 pts. wt. graphene in aqueous solution of sodium polyphosphate, sonicating, then adding 40-60 pts. wt. acidified modified nano bentonite, sodium polyphosphate carrying graphene and acidified modified nano-bentonite affinity between acidified nano-bentonite sheet, chip surface complex to form complex, taking graphene and nano-bentonite as carrier, stable, uniform load in nano-bentonite, filtering, washing and drying to obtain graphene-bentonite complex, and (ii) mixing graphene-bentonite complex and 100-200 pts. wt. organic solvent, then adding 20-30 pts. wt. phenol into mixed system, stirring, and then adding 1-3 pts. wt. surfactant, and dispersing by magnetic stirring. An INDEPENDENT CLAIM is also included for graphene mother liquor obtained by above method.