• 专利标题:   Preparing graphene comprises mixing graphite powder and aluminum chloride, heating, cooling, adding low-carbon nitroalkane and stirring to obtain intercalated mixture, heating using microwave, placing expanded graphite in water and stirring.
  • 专利号:   CN104085886-A, CN104085886-B
  • 发明人:   JI T, MA N, ZOU L
  • 专利权人:   JI T
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104085886-A 08 Oct 2014 C01B-031/04 201502 Pages: 10 Chinese
  • 申请详细信息:   CN104085886-A CN10363993 28 Jul 2014
  • 优先权号:   CN10363993

▎ 摘  要

NOVELTY - Preparing graphene comprises (i) mixing graphite powder and aluminum chloride, heating at 200-300 degrees C for 5-95 hours under inert gas protection, and cooling to 20-30 degrees C, (ii) adding low-carbon nitroalkane and stirring at 20-30 degrees C for 3-70 hours to obtain intercalated mixture, and (iii) heating intercalated mixture using microwave to obtain expanded graphite, placing expanded graphite in water and stirring to obtain graphene suspension. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The method: is simple, is easy to control and produces high quality graphene; and is environmentally friendly and suitable for large scale preparation. The graphene is convenient for storage and transportation. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene prepared by the above method.