• 专利标题:   Preparing of masterbatch for graphene-modified PVC composite material, by adding graphene powder to plasticizer solution, ultrasonically treating, adding PVC superfine powder and PVC paste resin ultrafine powder, crushing and dispersing.
  • 专利号:   CN110423415-A
  • 发明人:   LEI D, WUSEYINBAILA, YI H, MENGGENQIQIGE, SUN L, ZOU Y, DONG B, BAI H, JIN T, BAODUJIYA, LIU L, LI Y, JIAO R
  • 专利权人:   ERDOS REDBUD INNOVATION INST
  • 国际专利分类:   C08J003/22, C08K003/04, C08K005/12, C08L027/06
  • 专利详细信息:   CN110423415-A 08 Nov 2019 C08L-027/06 201990 Pages: 7 Chinese
  • 申请详细信息:   CN110423415-A CN10646363 17 Jul 2019
  • 优先权号:   CN10646363

▎ 摘  要

NOVELTY - Method for preparing of masterbatch for graphene-modified PVC composite material involves (i) adding graphene powder to the plasticizer solution, stirring for 20-120 minutes using ball mill or high-speed homogenizer, or carrying out ultrasonic treatment for 30-60 minutes using ultrasonic dispersion instrument to obtain 0.05-5% uniformly and stably dispersed graphene dispersion liquid, (ii) taking 50 pts. wt. graphene dispersion liquid, adding 0-20 pts. wt. PVC superfine powder and 30-50 pts. wt. PVC paste resin ultrafine powder, stirring for 0.5-2 hours using high-speed stirrer, and leaving still for more than 6 hours to obtain the graphene/PVC mixed slurry, and (iii) baking the graphene/PVC mixed slurry at 140-180 degrees C for 20-40 minutes, cooling to room temperature, crushing the graphene/PVC mixed slurry into particles using crusher to obtain the uniformly-dispersed master batch. USE - Method for preparing of masterbatch for graphene-modified PVC composite material. ADVANTAGE - The method is simple in process, environmentally-friendly and excellent in dispersibility, and has large application prospect.