• 专利标题:   Production method of graphene thermally conductive material involves adding raw materials into the material pretreatment component, solid raw materials are rolled into powder, intercept the impurities produced by mixing a variety of liquid raw materials, starting the mixing component.
  • 专利号:   CN114131783-A
  • 发明人:   ZHANG Z
  • 专利权人:   DONGGUAN MEIDI PLASTIC PIGMENT CO LTD
  • 国际专利分类:   B29B013/10, B29B007/12, B29B009/06, B29C048/78, C08K003/04, C08L101/00, C08L069/00
  • 专利详细信息:   CN114131783-A 04 Mar 2022 B29B-009/06 202253 Chinese
  • 申请详细信息:   CN114131783-A CN11463973 03 Dec 2021
  • 优先权号:   CN11463973

▎ 摘  要

NOVELTY - Production method of graphene thermally conductive material, which involves: i. adding the raw materials into the material pretreatment component (3), solid raw materials are rolled into powder, intercept the impurities produced by mixing a variety of liquid raw materials; ii. start the mixing component (2), stirring and mixing the pretreated solid and liquid raw materials in step 1, and heating them to form a mixture, heating temperature is 60-70 degreesC, stirring and mixing time is 20-30 minutes; iii. mixture obtained in step 2 is fed into the twin-screw granulator (4), and twin-screw granulator (4) and cooling assembly (5) are started successively, and mixture is extruded and granulated while being melt-mixed, surface of the twin-screw granulator (4) is cooled, and graphene thermally conductive material obtained by granulation will directly fall into the collection box (6) to complete the collection. USE - Production method of graphene thermally conductive material. ADVANTAGE - Production method of graphene thermally conductive material is not easy to deform, has good impact resistance, and ensures dimensional stability, not only pulverize solid raw materials to speed up mixing and melting, but also achieve the effect of separate delivery of solid and liquid raw materials. The impurities generated by mutual mixing are intercepted to ensure the quality of the finished product. In addition, during the operation of the twin-screw granulator, surface is also be cooled by water cooling, which further improves the service life of the twin-screw granulator. DETAILED DESCRIPTION - Production method of graphene thermally conductive material, which involves: i. adding the raw materials into the material pretreatment component (3) according to the mass ratio, the solid raw materials are rolled into powder, intercept the impurities produced by mixing a variety of liquid raw materials; ii. start the mixing component (2), stiring and mixing the pretreated solid and liquid raw materials in step 1, and heating them to form a mixture, heating temperature is 60-70 degreesC, stirring and mixing time is 20-30 minutes, and stirring mixing speed is 400-500 revolutions per minute; iii. mixture obtained in step 2 is fed into the twin-screw granulator (4), and twin-screw granulator (4) and cooling assembly (5) are started successively, and mixture is extruded and granulated while being melt-mixed, surface of the twin-screw granulator (4) is cooled, and graphene thermally conductive material obtained by granulation will directly fall into the collection box (6) to complete the collection. The material pretreatment component (3) in the step 1 includes a feeding hollow cylinder (31), fixing seat (32) and first motor (33). A support (34) is installed on the inner bottom of the feeding hollow cylinder (31), an integrated disc (35) is arranged at the center of the support member (34), a liquid feeding cylinder (36) is installed on the upper end of the disc (35). A solid material tray (37) is sleeved on the outer top of the liquid feeding cylinder (36). A ring plate (38) is rotatably connected to the upper edge of the feeding hollow cylinder (31). A first gear (39) is sleeved on the outer top of the ring plate (38). A first L-shaped plate (310) and a second L-shaped plate (311) are respectively installed on the inner top of the ring plate (38). A fixing seat (312) is installed on the bottom of the first L-shaped plate (310). A roller (313) is arranged inside the fixing seat (312). A sweeping brush (314) is connected to the bottom of the second L-shaped plate (311) by bolts. The power driving end of the first motor (33) is sleeved with a second gear (315) that meshes with the first gear (39). An INDEPENDENT CLAIM is also included for graphene thermal conductive material obtained by a production method for producing graphene thermally conductive material comprises 30-75 pts. wt. polymer matrix, 1-40 pts. wt. high thermal conductivity graphene, 10-20 pts. wt. graphite powder dispersion, 5-10 pts. wt. cycloaliphatic epoxy compound, 6-8 pts. wt. polycarbonate, 1-2 pts. wt. catalyst, 1-2 pts. wt. curing agent and 3-4 pts. wt. adhesive. DESCRIPTION OF DRAWING(S) - The drawing shows a structural schematic diagram of producing graphene thermal conductive material and preparation method. Mixing component (2) Material pretreatment component (3) Twin-screw granulator (4) Cooling assembly (5) Collection box (6)