• 专利标题:   Manufacture of nano graphene-based material used for e.g. rechargeable batteries, involves mixing graphite sulfuric slurry and potassium permanganate sulfuric solution and then adding aqueous hydrogen peroxide solution to mixture.
  • 专利号:   WO2011019095-A1, KR2011036721-A, CN102471068-A, US2012201738-A1, EP2493812-A1, KR1337970-B1, CN102471068-B, US8968695-B2, EP2493812-A4, EP2493812-B1
  • 发明人:   KWON Y J, KIM J H, GU J W, PARK W H, KIM S B, SHIN C M, JI B K, KWON D H, PARK S Y, JI B, GU J, KWON Y, PARK W, KWON D, SHIN C
  • 专利权人:   NBARO TECH CO LTD, NBARO TECH CO LTD, NBARO TECH CO LTD, IDT INT CO LTD, IDT INT CO LTD, STANDARD GRAPHENE CO LTD
  • 国际专利分类:   B82B003/00, C01B031/02, C01B031/04, B82Y040/00, B01J008/08, B01J008/18, B82Y030/00, C01B031/00, B01J019/00, B01J006/00, C01B032/05, C01B032/20
  • 专利详细信息:   WO2011019095-A1 17 Feb 2011 C01B-031/04 201123 Pages: 20 English
  • 申请详细信息:   WO2011019095-A1 WOKR004465 11 Aug 2009
  • 优先权号:   KR073152

▎ 摘  要

NOVELTY - Graphite flakes are mixed with sulfuric acid, to obtain graphite sulfuric slurry. Potassium permanganate is dissolved in sulfuric acid, to obtain potassium permanganate sulfuric solution. Graphite sulfuric slurry and potassium permanganate sulfuric solution are forced to flow into a lengthy micro-channel having inlet, reacting portion and outlet, and mixture is allowed to stand still in micro-channel at predetermined temperature. Then, aqueous hydrogen peroxide solution is added to reaction mixture, product is washed and dried, to obtain nano graphene-based material. USE - Manufacture of nano graphene-based material. Uses include but are not limited to polymeric composite, filler, rechargeable battery, transistor, super capacitor, hydrogen-storing container and biosensor. ADVANTAGE - The method economically and efficiently provides nano graphene-based material having excellent dispersibility and large surface area without causing explosion. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for equipment for producing nano graphene-based material equipment, which comprises graphite sulfuric slurry supply unit, potassium permanganate sulfuric solution supply unit, aqueous hydrogen peroxide solution supply unit, microreactor (8) including multiple microchannel modules surrounded by heat-exchangers, mixing unit for mixing reaction mixture discharged from the outlet of the micro-channel with aqueous hydrogen peroxide solution, washing unit and drying unit. DESCRIPTION OF DRAWING(S) - The drawing shows the schematic view of equipment for producing nano graphene-based material. Dosing pumps (3a,4a,3b,4b) Premixer (5,7) Microreactor (8) Hydrogen peroxide mixing tank (11)