• 专利标题:   Preparation of graphene in situ composite lithium iron manganese phosphate anode material involves mixing lithium, manganese, iron and phosphorus, adding lithium carbonate and phosphoric acid, grinding, drying and calcining.
  • 专利号:   CN110247044-A
  • 发明人:   LIU J, KONG J, LIN W, HUANG S, LI K, ZHANG X, XIONG W, FENG B, WANG Y, ZHANG H
  • 专利权人:   SHENZHEN EIGEN EQUATION GRAPHENE TECHNOL
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN110247044-A 17 Sep 2019 H01M-004/36 201978 Pages: 13 Chinese
  • 申请详细信息:   CN110247044-A CN10627997 11 Jul 2019
  • 优先权号:   CN10627997

▎ 摘  要

NOVELTY - Preparation of graphene in situ composite lithium iron manganese phosphate anode material comprises mixing lithium, manganese, iron and phosphorus at mole ratio of 1.0-1.5:0-1:0-1:1, adding lithium carbonate, manganous-manganic oxide, ferric oxide and phosphoric acid into mixed solvent, milling, adding polyethylene pyrrolidone and acetylene, and continuously grinding to obtain mixed solution; adding liquid oligomer C3 into obtained mixed solution, continuously grinding and mixing to obtain graphene compounded lithium iron manganese phosphate anode material slurry; drying obtained graphene compounded lithium iron manganese phosphate anode material slurry to obtain anode material precursor; and pre-heating anode material precursor under inert atmosphere, crushing, thinning and calcining. USE - Method for preparing graphene in situ composite lithium iron manganese phosphate anode material. ADVANTAGE - The method is safe, can obtain product with good structural stability and improved cycle life performance.