• 专利标题:   Preparing graphene-based photocatalyst material involves adding lanthanum chloride into anhydrous ethanol, adding titanium source and stirring to obtain solution, and adding solution into reactor and carrying out aeration reaction.
  • 专利号:   CN107020073-A
  • 发明人:   ZHU Y
  • 专利权人:   XIAOGAN SHUANGHUA APPLIED TECHNOLOGY DEV
  • 国际专利分类:   B01J021/06, B01J021/18, B01J023/10, B01J037/34
  • 专利详细信息:   CN107020073-A 08 Aug 2017 B01J-023/10 201766 Pages: 9 Chinese
  • 申请详细信息:   CN107020073-A CN10311451 05 May 2017
  • 优先权号:   CN10311451

▎ 摘  要

NOVELTY - Preparing graphene-based photocatalyst material involves adding lanthanum chloride into anhydrous ethanol, adding titanium source and stirring to obtain solution. The solution is added into the reactor and aeration reaction is carried out for 2-5 hours. the reaction mixture is sealed and reacted for 10-15 hours. The reaction mixture is naturally cooled and filtered to obtain mixed precipitate. The mixed precipitate is mixed with dispersant and graphene powder, and ultrasonically dispersed for 2 to 4 hours. USE - Method for preparing graphene-based photocatalyst (claimed). ADVANTAGE - The method enables to prepare graphene-based photocatalyst material which has reduced the defect of graphene, increased the graphene and perovskite nano material absorption efficiency. DETAILED DESCRIPTION - Preparing graphene-based photocatalyst material involves adding lanthanum chloride into anhydrous ethanol, adding titanium source and stirring to obtain solution. The solution is added into the reactor and aeration reaction is carried out for 2-5 hours. the reaction mixture is sealed and reacted for 10-15 hours. The reaction mixture is naturally cooled and filtered to obtain mixed precipitate. The mixed precipitate is mixed with dispersant and graphene powder, and ultrasonically dispersed for 2 to 4 hours to obtain dispersion precursor. The dispersion precursor is placed in the photoreactor and reacted for 2 to 5 hours and filtered to obtain desired product.