• 专利标题:   Preparing manganese dioxide/graphene nanocomposite used as modified electrode for detecting caffeic acid in beverages, involves mixing mesoporous carbon with potassium permanganate and deionized water to obtain suspension.
  • 专利号:   CN106115787-A, CN106115787-B
  • 发明人:   LI J, TONG C, LIU M, ZHANG F, XU Z
  • 专利权人:   UNIV HENGYANG NORMAL
  • 国际专利分类:   C01G045/02, G01N027/30
  • 专利详细信息:   CN106115787-A 16 Nov 2016 C01G-045/02 201705 Pages: 13 Chinese
  • 申请详细信息:   CN106115787-A CN10442311 21 Jun 2016
  • 优先权号:   CN10442311

▎ 摘  要

NOVELTY - Preparing manganese dioxide/graphene nanocomposite involves mixing mesoporous carbon with potassium permanganate and deionized water with stirring for 8-24 hours to obtain suspension which is mixed with concentrated sulfuric acid with stirring for 0.5-3 hours to obtain a mixture. The mixture is heated to 70-90 degrees C for 0.5-3 hours to obtain the reaction solution. The reaction solution is diluted with deionized water, cooled to room temperature and precipitated. The resulting solution is filtered to obtain precipitate which is washed and dried to obtain manganese dioxide/graphene nanocomposite. USE - Method for preparing manganese dioxide/graphene nanocomposite which is used as modified electrode used for detecting caffeic acid in beverages, food and medicine (claimed). ADVANTAGE - The method enables to prepare manganese dioxide/graphene nanocomposite which has good stability and high sensitivity. The electrode prepared using manganese dioxide/graphene nanocomposite has low detection limit and strong anti-interference performance.