• 专利标题:   Preparing high dispersion multi-stage porous titanium based selective catalytic reduction catalyst comprises e.g. adding carrier, active auxiliary agent, binder, water and ammonia water, stirring, heating, introducing raw material to extruder for extrusion forming, drying and calcining.
  • 专利号:   CN114392730-A
  • 发明人:   CUI J, ZHANG X, LUO S, PENG Y, YU X, MU B
  • 专利权人:   HENAN KANGNINGTE ENVIRONMENTAL PROTECTIO
  • 国际专利分类:   B01D053/56, B01D053/86, B01J021/06, B01J021/18, B01J023/28, B01J023/30, B01J023/652, B01J023/881, B01J023/882, B01J023/885, B01J023/887, B01J023/888, B01J023/89
  • 专利详细信息:   CN114392730-A 26 Apr 2022 B01J-021/18 202260 Chinese
  • 申请详细信息:   CN114392730-A CN10025920 11 Jan 2022
  • 优先权号:   CN10025920

▎ 摘  要

NOVELTY - Preparing high dispersion multi-stage porous titanium (Ti) based selective catalytic reduction (SCR) catalyst comprises adding 40-50 pts. wt. carrier, 2-6 pts. wt. active auxiliary agent or precursor of auxiliary agent, 2-4 pts. wt. binder, water and ammonia water with a mass concentration of 20% into the stirring device at a speed of 4000 revolutions/minute, stirring for 0.5-1 hour, and placing in a mixer for 0.5-1 hour at a speed of 7000 revolutions/minute, adding 5-10 pts. wt. carrier, water and ammonia water, and stirring at a speed of 4000 revolutions/minute for 0.5-1 hour, mixing at 7000 revolutions/minute for 0.5-1 hour, heating to 100degreesC for 0.5-1 hour, introducing the raw material to extruder for extrusion forming, extruding porous number is 10-40 holes of honeycomb catalyst, drying for 5-15 days at 25-60degreesC, and calcining for 24-72 hours at 480-600degreesC. USE - The method is useful for preparing high dispersion multi-stage porous titanium based selective catalytic reduction catalyst. ADVANTAGE - The catalyst has multiple active sites. DETAILED DESCRIPTION - Preparing high dispersion multi-stage porous titanium (Ti) based selective catalytic reduction (SCR) catalyst comprises (i) adding 40-50 pts. wt. carrier, 2-6 pts. wt. active auxiliary agent or precursor of auxiliary agent, 2-4 pts. wt. binder, water and ammonia water with a mass concentration of 20% into the stirring device at a speed of 4000 revolutions/minute, stirring for 0.5-1 hour, and placing in a mixer for 0.5-1 hour at a speed of 7000 revolutions/minute, (ii) adding 5-10 pts. wt. carrier, water and ammonia water with a mass concentration of 20% to the raw materials, and stirring at a speed of 4000 revolutions/minute for 0.5-1 hour, and mixing at a speed of 7000 revolutions/minute for 0.5-1 hour, (iii) adding 5-10 pts. wt. carrier, water and ammonia water with a mass concentration of 20% to the raw materials, and stirring at a speed of 4000 revolutions/minute for 0.5-1 hour, mixing at 7000 revolutions/minute for 0.5-1 hour, heating to 100degreesC for 0.5-1 hour, (iv) adding 0.5-5 pts. wt. active substances, 10-20 pts. wt. prefabricated materials, 5-8 pts. wt. extrusion agent, mixing for 0.2-0.5 hour with 4000 revolutions/minute rotating speed reversing mixing machine, mixing for 0.2-0.5 hour until the water content of the mixing raw material is 25-30%, the pH is 7.5-8, and stopping mixing, and (5) introducing the raw material to the extruder for extrusion forming, extruding porous number is 10-40 holes of honeycomb catalyst, drying for 5-15 days at 25-60degreesC, and calcining for 24-72 hours at 480-600degreesC.