• 专利标题:   Preparing graphene composite conductive paste used as electrode conductive agent in lithium-ion battery, involves ball milling on graphene oxide solution obtained from graphite, drying to obtain graphene powder, mixing graphene powder with conductive agent.
  • 专利号:   CN113745518-A
  • 发明人:   MA T, CHEN X, LI F, ZHI F, WANG J, LIU A, LIU S, CHEN D, YI S
  • 专利权人:   JINCHUAN GROUP CO LTD
  • 国际专利分类:   H01B001/04, H01M010/0525, H01M004/62
  • 专利详细信息:   CN113745518-A 03 Dec 2021 H01M-004/62 202211 Chinese
  • 申请详细信息:   CN113745518-A CN10980811 25 Aug 2021
  • 优先权号:   CN10980811

▎ 摘  要

NOVELTY - The preparation method of the graphene composite conductive paste involves: (a) preparing graphene oxide solution from graphite through strong acid oxidation by a Brodie method, then performing ultrasonic and ball milling on the graphene oxide solution, and drying the graphene oxide solution to obtain graphene powder; (b) stirring and mixing the graphene powder and a conductive agent at a speed of 500-800 revolutions per minute for 1-2 hours; (c) premixing a dispersant and a solvent to obtain a mixed solution; and (d) adding the mixture from the step (b) into the solution obtained from the step (c), fully mixing and stirring, and then adding into a homogenizing grinding dispersion machine for fine grinding and dispersion. The dispersant is polyvinylpyrrolidone, polyvinyl alcohol or sodium dodecyl benzene sulfonate. The solvent is N-methyl pyrrolidone, deionized water, ethanol or N-N dimethyl acetamide. USE - Preparation method of graphene composite conductive slurry used as electrode conductive agent in lithium-ion battery. ADVANTAGE - The method is simple and provides graphene composite conductive slurry with excellent product performance.