• 专利标题:   Preparing nitro compounds by solid acid nitration of aromatic hydrocarbon compounds, involves nitration reaction of aromatic hydrocarbon compounds and carrying out nitric acid in tubular reactor filled with solid acid catalyst, and subjecting nitration reaction product to alkali washing.
  • 专利号:   CN114349643-A
  • 发明人:   JIN G, ZHANG R, HUANG W, ZHAO S, REN L, JI F, YANG Z
  • 专利权人:   CHINA PETROLEUM CHEM CORP, SINOPEC NANJING CHEM RES INST CO LTD
  • 国际专利分类:   B01J027/053, B01J035/10, C07C201/08, C07C205/06, C07C205/12
  • 专利详细信息:   CN114349643-A 15 Apr 2022 C07C-205/06 202251 Chinese
  • 申请详细信息:   CN114349643-A CN11090704 13 Oct 2020
  • 优先权号:   CN11090704

▎ 摘  要

NOVELTY - Preparing nitro compounds by solid acid nitration of aromatic hydrocarbon compounds involves nitration reaction of aromatic hydrocarbon compounds and carrying out nitric acid in a tubular reactor filled with solid acid catalyst, and subjecting the nitration reaction product to alkali washing, water washing and refining to obtain nitro compounds. USE - Method for preparing nitro compounds by solid acid nitration of aromatic hydrocarbon compounds. ADVANTAGE - The method is simple, realize continuous stable production of aromatic compound. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic structural diagram of a nitration reaction tube reactor. Reactor shell (1) Cooling agent inlet (2) Heat exchange tube (3) Cooling agent distributing pipe (4) Cooling agent distributing pipe (5) Reactor shell (6) Heat exchange tube (7) Coolant outlet (8) Material outlet (9) Solid acid catalyst (10)