• 专利标题:   Preparation of graphene oxide surface graft-modified aramid fiber involves providing tris hydrochloride solution buffer solution, adding aminated graphene oxide, dipping dopamine modified aramid fiber in obtained solution, and reacting.
  • 专利号:   CN104047160-A, CN104047160-B
  • 发明人:   XIE Z, LIU Y, WU S, DONG Q
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   D06M011/74
  • 专利详细信息:   CN104047160-A 17 Sep 2014 D06M-011/74 201481 Pages: 8 Chinese
  • 申请详细信息:   CN104047160-A CN10269027 17 Jun 2014
  • 优先权号:   CN10269027

▎ 摘  要

NOVELTY - Preparation of graphene oxide surface graft-modified aramid fiber involves providing tris hydrochloride solution having pH of 8.5, adding aminated graphene oxide, dipping dopamine modified aramid fiber in the obtained solution, and reacting at 15-50 degrees C for 10-24 hours. The aminated graphene oxide is obtained by adding graphene oxide in aqueous solution, obtaining graphene oxide suspension, ultrasonic processing for 30-60 minutes, adding amine reducing agent at 3-100 degrees C, mechanically stirring for 6-24 hours, cleaning, and drying. USE - Preparation of graphene oxide surface graft-modified aramid fiber (claimed). ADVANTAGE - The graphene oxide surface graft-modified aramid fiber having excellent adhesiveness and uniform surface is prepared by simple method. DETAILED DESCRIPTION - Preparation of graphene oxide surface graft modified aramid fiber involves providing tris hydrochloride solution having pH of 8.5, adding aminated graphene oxide, dipping dopamine modified aramid fiber in the obtained solution, and reacting at 15-50 degrees C for 10-24 hours. The aminated graphene oxide is obtained by adding graphene oxide in aqueous solution, obtaining graphene oxide suspension, ultrasonically processing for 30-60 minutes, adding amine reducing agent at 3-100 degrees C, mechanically stirring for 6-24 hours, cleaning, and drying. The dopamine-modified aramid fiber is obtained by providing tris hydrochloride solution, adding dopamine hydrochloride, dipping aramid fiber in the dopamine solution for 10-24 hours, cleaning using deionized water, and drying.