• 专利标题:   Graphene film-based low-frequency sound wave detector comprises detector signal collecting portion comprises graphene film and conductive substrate with graphene film.
  • 专利号:   CN108871547-A
  • 发明人:   GAO C, PENG L, LIU Y, GUO Y
  • 专利权人:   HANGZHOU GAOXI TECHNOLOGY CO LTD, UNIV ZHEJIANG
  • 国际专利分类:   C01B032/184, C01B032/194, G01H011/06
  • 专利详细信息:   CN108871547-A 23 Nov 2018 G01H-011/06 201911 Pages: 11 Chinese
  • 申请详细信息:   CN108871547-A CN10753777 10 Jul 2018
  • 优先权号:   CN10753777

▎ 摘  要

NOVELTY - A graphene film-based low-frequency sound wave detector comprises detector signal collecting portion comprises graphene film and conductive substrate with graphene film at thickness of 20-50 nm and crosslinking degree of 1-5%. The graphene film is prepared by preparing 4 mg/mL graphene oxide aqueous solution, adding 10-50 wt.% fumed nitric acid, heating and refluxing at 100-120 degrees C for 1-6 hours, centrifuging and washing, obtaining porous graphene oxide, preparing into 0.5-10 mu g/mL aqueous solution, filtering to obtain film, attaching onto substrate, fuming at 80-100 degrees C for 0.1-1 hour, coating with solid transfer agent, cooling, performing heat treatment, sputtering with 30 wt.% metal titanium, molybdenum or cobalt metal, chlorinating at 800-1200 degrees C, sintering at 1500 degrees C at rate of 5-20 degrees C/minute, and raising temperature to 2000 degrees C at rate of 2-5 degrees C/minute. USE - Graphene film-based low-frequency sound wave detector. ADVANTAGE - The graphene film has controllable conductivity and has adjustable intensity.