• 专利标题:   Preparation of graphene involves mixing crystalline flake graphite, concentrated nitric acid, and potassium permanganate, adding phosphoric acid, reacting, washing, drying, extruding, cooling, and adding aqueous sodium bicarbonate.
  • 专利号:   CN103950927-A, CN103950927-B
  • 发明人:   JIN C, YANG X
  • 专利权人:   SUZHOU SDIK NEW MATERIAL TECHNOLOGY CO, SUZHOU SIDIKE NEW MATERIALS SCI TECHNO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103950927-A 30 Jul 2014 C01B-031/04 201468 Pages: 5 Chinese
  • 申请详细信息:   CN103950927-A CN10216178 21 May 2014
  • 优先权号:   CN10216178

▎ 摘  要

NOVELTY - A graphene is prepared by mixing crystalline flake graphite, concentrated nitric acid, and potassium permanganate to obtain mixed acid solution, adding phosphoric acid, reacting at 85-95 degrees C for 1 hour, washing until pH is 4.5-5.5, drying at less than or equal to 100 degrees C, extruding at 550-900 degrees C for 30 s to 2 minutes, cooling at room temperature, adding aqueous sodium bicarbonate, stirring at 100-270 degrees C for 10 minutes to 3 hours, and drying under vacuum state for 12-24 hours. USE - Preparation of graphene (claimed). ADVANTAGE - Preparation process has greatly reduced process temperature.