• 专利标题:   Preparing fluorinated graphene useful e.g. in lithium battery electrode materials comprises e.g. preparing graphite oxide, stirring water and graphene oxide, starting ultrasound and microwave, and adding fluorine-containing compound.
  • 专利号:   CN104860289-A, CN104860289-B
  • 发明人:   LONG D, TAN B
  • 专利权人:   HUNAN ELEMENT PASSWORD GRAPHENE RES INST, HUNAN YUANSU MIMA GRAPHENE HIGHTECHNOLO
  • 国际专利分类:   C01B031/00, C01B032/10, C01B032/19
  • 专利详细信息:   CN104860289-A 26 Aug 2015 C01B-031/00 201578 Pages: 9 Chinese
  • 申请详细信息:   CN104860289-A CN10192820 22 Apr 2015
  • 优先权号:   CN10192820

▎ 摘  要

NOVELTY - Preparing fluorinated graphene comprises (i) preparing graphite oxide using graphene, (ii) adding 600 ml water in a storage tank of a fluorinated graphene preparation device, and then adding the graphene oxide, (iii) starting ultrasound and microwave, adding 8-17 g fluorine-containing compound, heating to 80 degrees C, stirring for 3 hours, and naturally cooling to room temperature to obtain reaction product, and (iv) conducting press filtration washing on the reaction product to reach a pH value of 7, and spray-drying to obtain the fluorinated graphene powder. USE - The fluorinated graphene is useful: in lithium battery electrode materials, lubrication materials, or medicine, catalysis or coating materials (claimed). ADVANTAGE - The method: is simple and pollution-free; and has short preparation time, low cost and high production yield. The fluorinated graphene can be directly used as or synthesized into a wear resistant material of engine cylinder.