• 专利标题:   Preparation of functionalized graphene oxide, e.g. for electronic device, by grinding graphite oxide, mixing with a solvent, carrying out ultrasonic treatment, centrifuging, carrying out dialysis, reacting with ammonia water, and drying.
  • 专利号:   CN102689896-A, CN102689896-B
  • 发明人:   HOU B, JIA L, LI D, SUN Y, WANG G
  • 专利权人:   CHINESE ACAD SCI SHANXI INST COAL CHEM, CHINESE ACAD SCI COAL CHEM INST
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102689896-A 26 Sep 2012 C01B-031/04 201322 Pages: 9 Chinese
  • 申请详细信息:   CN102689896-A CN10067653 15 Mar 2012
  • 优先权号:   CN10067653

▎ 摘  要

NOVELTY - Preparation of a functionalized graphene oxide comprises preparing a graphene oxide sol by grinding graphite oxide to a fine powder of 1-100 mu m, mixing with a solvent, stirring for 0.5-10 hours to form 0.25-5 mg/mL suspension, carrying out ultrasonic treatment for 0.5-2 hours at 40-100 W, centrifuging for 0.5-3 hours at not less than 3000 revolutions/minute to remove dregs, and carrying out dialysis; and reacting the graphene oxide sol with 25-28 wt.% ammonia water at a volume ratio of 5-50:1 for 0.5-10 hours at 40-180 degrees C under sealing condition, and drying at 20-28 degrees C. USE - Method for the preparation of a functionalized graphene oxide used for an electronic device, a composite material, a battery, a field emitter, a gas sensor, a catalytic, and an energy storage material. ADVANTAGE - The method has mild conditions and low energy consumption.