• 专利标题:   Method for preparing nickel cobaltite/nitrogen-doped graphene composite material for supercapacitor electrode material, involves dissolving cobalt chloride hexahydrate, nickel chloride hexahydrate and urea in water followed by stirring.
  • 专利号:   CN110189921-A
  • 发明人:   LIN H, LIU S, HU X, CHEN J, LIU Y, YIN S, YANG T, HAN S
  • 专利权人:   SHANGHAI INST TECHNOLOGY
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/32, H01G011/46, H01G011/86
  • 专利详细信息:   CN110189921-A 30 Aug 2019 H01G-011/24 201976 Pages: 8 Chinese
  • 申请详细信息:   CN110189921-A CN10469004 31 May 2019
  • 优先权号:   CN10469004

▎ 摘  要

NOVELTY - A nickel cobaltite/nitrogen-doped graphene composite material preparing method involves dissolving cobalt chloride hexahydrate, nickel chloride hexahydrate and urea in deionized water, stirring the mixture uniformly, forming a solution having an atomic molar ratio of cobalt to nickel of 1:1.5-1:2.5. A graphene oxide is added to ethanol to obtain a graphene oxide dispersion, where the content of graphene oxide is 0.5-1 mg/mL and dosage of graphene oxide is 25 mg graphene oxide/1 mmol of nickel chloride hexahydrate. The obtained solution is added to the graphene oxide dispersion, ammonia water is added to bring the pH to 10 and stirred to obtain a precursor suspension. The precursor suspension is transferred to an autoclave for hydrothermal reaction at 120-180 degrees C for 6-12 hours and cooled to room temperature to obtain a reaction liquid. The obtained reaction liquid is washed with water and ethanol, and lyophilized to obtain the finished product. USE - Method for preparing a nickel cobaltite/nitrogen-doped graphene composite material for supercapacitor electrode material (claimed). ADVANTAGE - The method enables preparing the nickel cobaltite/nitrogen-doped graphene composite material with uniform particle size and better electrochemical performance in one-step, and simple manner. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a supercapacitor electrode material.