• 专利标题:   Method for preparing high concentration graphene-polyaniline nano fiber compound dispersion, involves adding oxidized graphite alkene and polyaniline nanometer fiber in distilled water to obtain graphene oxide dispersion liquid.
  • 专利号:   CN102321254-A, CN102321254-B
  • 发明人:   HE W, JING X, LI Y, ZHANG W
  • 专利权人:   UNIV XIAN JIAOTONG
  • 国际专利分类:   C01B031/04, C08J003/03, C08J005/18, C08K003/04, C08L079/02
  • 专利详细信息:   CN102321254-A 18 Jan 2012 C08J-003/03 201306 Chinese
  • 申请详细信息:   CN102321254-A CN10293397 30 Sep 2011
  • 优先权号:   CN10293397

▎ 摘  要

NOVELTY - A high concentration graphene-polyaniline nano fiber compound dispersion preparing method involves adding oxidized graphite alkene for preparing polyaniline nano fiber dispersing graphite oxide and polyaniline nanometer fiber in distilled water to obtain graphene oxide dispersion liquid and polyaniline nano fiber dispersion liquid. A reducing agent is added to the composite dispersion liquid. The obtained product is reacted for 2-4 hours to obtain graphene under the ultrasonicpolyaniline nanometer fiber composite dispersion. USE - Method for preparing high concentration graphene-polyaniline nano fiber compound dispersion. ADVANTAGE - The method ensures synergetic effect of the high concentration graphene-polyaniline nano fiber compound dispersion. The high concentration graphene-polyaniline nano fiber compound dispersion has better flexibility and high conductivity. DETAILED DESCRIPTION - A high concentration graphene-polyaniline nano fiber compound dispersion preparing method involves adding oxidized graphite alkene for preparing polyaniline nano fiber dispersing graphite oxide and polyaniline nanometer fiber in distilled water and ultrasonically dispersing the obtained product to obtain graphene oxide dispersion liquid with concentration of 0.5 -2 milligram per milliliter and polyaniline nano fiber dispersion liquid with concentration of 0.1-0.3 milligram per milliliter, where a mass ratio of polyaniline nano fiber to the graphene oxide is 1-4:1. The graphene oxide dispersing liquid is dropped to the polyaniline nanometer fiber dispersion liquid and continuously and ultrasonically dispersed to the obtained product, where pH of the obtained product is regulated at 4 degrees C to obtain graphene-polyaniline nanometer fiber dispersion liquid with concentration of 0.5-1 milligram per milliliter. The high-concentration graphene-polyaniline nanometer fiber composite dispersion liquid is maintained at 50-80 degrees C under protection of nitrogen. A reducing agent is added to the composite dispersion liquid. The obtained product is reacted for 2-4 hours to obtain graphene under the ultrasonicpolyaniline nanometer fiber composite dispersion, where mass ratio of the graphene oxide and reducing agent is 10:5-9.