• 专利标题:   Preparation of composite antibiotic-degrading photocatalyst used for treating antibiotic-containing wastewater, includes mixing graphene oxide and deionized water and performing ultrasonic dispersion.
  • 专利号:   CN104941621-A, CN104941621-B
  • 发明人:   DANG Z, HUANG Y, MA T, YANG C, ZENG X
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY, UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   B01J021/18, C02F001/30
  • 专利详细信息:   CN104941621-A 30 Sep 2015 B01J-021/18 201605 Pages: 10 Chinese
  • 申请详细信息:   CN104941621-A CN10278124 26 May 2015
  • 优先权号:   CN10278124

▎ 摘  要

NOVELTY - Preparation of composite antibiotic degrading photocatalyst involves mixing graphene oxide and deionized water, stirring, performing ultrasonic dispersion, mixing titanium oxide to sodium hydroxide solution in reaction vessel, stirring to dissolve, transferring to hydrothermal reaction kettle, cooling, washing, drying to obtain titanium oxide nanowire, adding to graphene oxide dispersion, mixing for 2-6 hours, sonicating for 1-3 hours, adding absolute ethanol, transferring to hydrothermal reaction kettle heating at 120-125 degrees C, washing crude product, centrifuging, drying and calcining. USE - Method for preparing composite antibiotic-degrading photocatalyst used for treating antibiotic-containing wastewater (claimed). ADVANTAGE - The method is environmental-friendly and has high efficiency. It has low operational cost, short degradation time, low feed ratio and advanced technology. It is suitable for low concentration antibiotic. DETAILED DESCRIPTION - Preparation of composite antibiotic-degrading photocatalyst involves mixing graphene oxide and deionized water, stirring, performing ultrasonic dispersion, mixing titanium oxide to sodium hydroxide solution in reaction vessel, stirring to dissolve, transferring to hydrothermal reaction kettle, cooling, washing, drying to obtain titanium oxide nanowire, adding to graphene oxide dispersion, mixing for 2-6 hours, sonicating for 1-3 hours, adding absolute ethanol, transferring to hydrothermal reaction kettle heating at 120-125 degrees C, washing crude product, centrifuging, drying to obtain graphene oxide-titanium oxide composite wire, calcining at 600-900 degrees C under inert gas or vacuum, milling and sieving. The mass ratio of absolute ethanol to graphene is 40-80:1.