• 专利标题:   Preparing magnetic trisalt/cobalt hydroxide/reduced graphene ternary heterojunction photocatalyst involves dispersing graphene oxide in mixture of ethanol and water in certain ratio in solvent to obtain graphene oxide dispersion.
  • 专利号:   CN107413343-A
  • 发明人:   YU H, LI H
  • 专利权人:   NORTHEAST INST GEOGRAPHY AGRIC ECOLOGY
  • 国际专利分类:   B01J021/18, B01J023/75
  • 专利详细信息:   CN107413343-A 01 Dec 2017 B01J-023/75 201804 Pages: 17 Chinese
  • 申请详细信息:   CN107413343-A CN10370306 23 May 2017
  • 优先权号:   CN10370306

▎ 摘  要

NOVELTY - Preparing magnetic trisalt/cobalt hydroxide/reduced graphene ternary heterojunction photocatalyst involves dispersing graphene oxide in a mixture of ethanol and water in ratio of 1:(4-6) solvent to obtain graphene oxide dispersion, adding cetyltrimethylammonium bromide into graphene oxide dispersion, stirring, adding sodium hydroxide and cobalt nitrate hexahydrate, and stirring for 0.5-2 hours to obtain a mixed solution. USE - Method for preparing magnetic trisalt/cobalt hydroxide/reduced graphene ternary heterojunction photocatalyst (claimed). ADVANTAGE - The method enables to prepare magnetic trisalt/cobalt hydroxide/reduced graphene ternary heterojunction photocatalyst is recycled, which has high contains 25 wt.% of reducing graphene oxide light catalyst, saves time, and has better catalytic activity than the existing cobalt-based catalyst. DETAILED DESCRIPTION - Preparing magnetic trisalt/cobalt hydroxide/reduced graphene ternary heterojunction photocatalyst involves dispersing graphene oxide in a mixture of ethanol and water in ratio of 1:(4-6) solvent to obtain graphene oxide dispersion, adding cetyltrimethylammonium bromide into graphene oxide dispersion, stirring, adding sodium hydroxide and cobalt nitrate hexahydrate, and stirring for 0.5-2 hours to obtain a mixed solution. The mixed solution is transferred to a teflon reactor, reaction is performed at 150-170 degrees C for 3-5 hours to obtain reactant. The obtained reactant is centrifuged to obtain a precipitate. The precipitate is washed and dried to obtain final product.