• 专利标题:   Preparing graphene used for sensor by dispersing graphene oxide in water, adding soluble high molecular polymer to the graphene oxide dispersion and adding guanidine hydrochloride to polymer and graphite oxide mixed solution to react.
  • 专利号:   CN104261393-A, CN104261393-B
  • 发明人:   DONG C, GUO Y, MA Q, SHUANG S, SONG J
  • 专利权人:   UNIV SHANXI DATONG, UNIV DATONG
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104261393-A 07 Jan 2015 C01B-031/04 201518 Pages: 8 Chinese
  • 申请详细信息:   CN104261393-A CN10490875 24 Sep 2014
  • 优先权号:   CN10490875

▎ 摘  要

NOVELTY - Preparing graphene comprises: (1) dispersing graphene oxide in water to obtain a uniform dispersion of graphene oxide; (2) adding soluble high molecular polymer to the graphene oxide dispersion to obtain a mixed solution of high molecular polymer and graphite oxide; (3) adding guanidine hydrochloride to the obtained mixed solution, and adding alkaline solution to regulate the pH value to 8-12, placing the obtained product in an oil bath pan, stirring the reaction product at 60-100 degrees C for 1-5 hours, followed by centrifuging and washing. USE - The method is useful for preparing graphene (claimed), which is useful for sensor and electric device. ADVANTAGE - The method is capable of simply and easily preparing the graphene with less equipment usage. DETAILED DESCRIPTION - Preparing graphene comprises: (1) dispersing graphene oxide in water to obtain a uniform dispersion of graphene oxide; (2) adding soluble high molecular polymer to the graphene oxide dispersion to obtain a mixed solution of high molecular polymer and graphite oxide; (3) adding guanidine hydrochloride to the obtained mixed solution, where the mass ratio of guanidine hydrochloride and graphene oxide is 10:1-100:1, and adding alkaline solution to regulate the pH value to 8-12, placing the obtained product in an oil bath pan, stirring the reaction product at 60-100 degrees C for 1-5 hours, followed by centrifuging and washing.