• 专利标题:   Manufacture of ultra-high-strength graphene-modified polymer material involves mixing graphene oxide solution, chitosan-acetic acid solution, carbon fiber-based dispersed solution, and crosslinking agent, melt-extruding, and granulating.
  • 专利号:   CN109021522-A
  • 发明人:   ZHANG C
  • 专利权人:   JINAN DEV ZONE XINGHUO TECHNOLOGY RES
  • 国际专利分类:   C08L067/04, C08L033/02, C08L005/08, C08K013/04, C08K007/06, C08K003/04, C08K005/07
  • 专利详细信息:   CN109021522-A 18 Dec 2018 C08L-067/04 201920 Pages: 5 Chinese
  • 申请详细信息:   CN109021522-A CN10751110 10 Jul 2018
  • 优先权号:   CN10751110

▎ 摘  要

NOVELTY - Manufacture of ultra-high-strength graphene-modified polymer material involves adding graphene oxide to deionized water, ultrasonically dispersing for 2-3 hours to obtain uniformly dispersed aqueous graphene oxide solution having a concentration of 5-10 wt.%, adding chitosan to 0.5-2 wt.% acetic acid solution, magnetically stirring to obtain a chitosan-acetic acid solution, adding 3-aminopropyltriethoxysilane, carbon fibers, and dicyclohexylcarbodiimide to a solvent, magnetically stirring for 4-6 hours, uniformly dispersing to obtain a dispersed solution (a), adding the chitosan acetic acid solution and the dispersed solution (a) to the aqueous graphene oxide solution, magnetically stirring, adding a crosslinking agent, and ultrasonically treating for 20-30 minutes, heating to 80-90 degrees C for 5-8 hours, stirring, adding polyacrylic acid and polylactic acid, mixing for 1-2 hours, uniformly mixing, adding the mixture to a twin-screw extruder, melt-extruding, granulating, and drying. USE - Manufacture of ultra-high-strength graphene-modified polymer material. ADVANTAGE - The method enables manufacture of ultra-high-strength graphene-modified polymer material with excellent strength and thermal stability, and suppressed agglomeration phenomenon.