• 专利标题:   Preparing lanthanum-based oxide composite nano material comprises e.g. adding lanthanum(III) nitrate hexahydrate, nitrate and graphene oxide to N,N-dimethylformamide, mixing and stirring, then heating, calcining, grinding, and freeze-drying.
  • 专利号:   CN112225264-A
  • 发明人:   DAI H, LI Z, LIU H, GUO D, SUN M, CHEN J, SHANG J, WEI M
  • 专利权人:   UNIV ZHENGZHOU LIGHT IND
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01F017/10, C01F017/229, C01G053/04, H01G011/24, H01G011/30, H01G011/46
  • 专利详细信息:   CN112225264-A 15 Jan 2021 C01G-053/04 202114 Pages: 14 Chinese
  • 申请详细信息:   CN112225264-A CN11076907 10 Oct 2020
  • 优先权号:   CN11076907

▎ 摘  要

NOVELTY - Preparing lanthanum-based oxide composite nano material, comprises (i) adding lanthanum(III) nitrate hexahydrate, nitrate and graphene oxide into N,N-dimethylformamide, and mixing and stirring for 2 hours, (ii) adding polyvinylpyrrolidone K-30 under low-speed magnetic stirring condition, mixing uniformly, stirring and heating the solution to boil, reducing the heating temperature when the solution evaporates to 1/3 of the original solution volume, and continuously stirring until the solution becomes colloid, and (iii) transferring the product prepared in step (ii) into a quartz boat, then placing in a muffle furnace for high-temperature calcining, reacting completely, taking out, grinding into powder, and freeze-drying to obtain final product. USE - The lanthanum-based oxide composite nano material is useful for electrochemical energy storage devices, preferably supercapacitor (claimed). ADVANTAGE - The method: has simple process and low cost; and is suitable for industrial production.