• 专利标题:   Preparation of chromic oxide-graphene nano sheet material used in lithium ion battery material field, involves dispersing graphene and chromate in aqueous-alcoholic solution, transferring mixture, filtering, washing and drying.
  • 专利号:   CN103151501-A, CN103151501-B
  • 发明人:   LI J, ZHAO G, WANG X
  • 专利权人:   PLASMA PHYSICS INST CHINESE ACAD SCI
  • 国际专利分类:   B82Y040/00, H01M004/36
  • 专利详细信息:   CN103151501-A 12 Jun 2013 H01M-004/36 201379 Pages: 8 Chinese
  • 申请详细信息:   CN103151501-A CN10043761 02 Feb 2013
  • 优先权号:   CN10043761

▎ 摘  要

NOVELTY - Preparation of chromic oxide-graphene nano sheet material involves uniformly dispersing graphene and chromate in pure water or aqueous-alcoholic solution, stirring, obtaining homogeneous solution, obtaining mixture, transferring obtained mixture to hydrothermal reaction kettle, reacting, filtering, washing and drying the product, obtaining chromium hydroxide hydrate nanosheet, calcining obtained chromium hydroxide hydrate oxide nanosheet under protection of argon gas or other inert gas. USE - Preparation of chromic oxide-graphene nano sheet material used in lithium ion battery material field. ADVANTAGE - The chromic oxide-graphene nano sheet material is economically prepared with high purity and specific surface area without polluting the environment, by a simple method. DETAILED DESCRIPTION - Preparation of chromic oxide-graphene nano sheet material involves uniformly dispersing 0.2-10 parts mass graphene and 1000-5000 parts mass chromate in pure water or aqueous-alcoholic solution, stirring for 0.5-24 hours, obtaining homogeneous solution, adjusting pH value to 1-8, stirring, obtaining mixture, transferring obtained mixture to hydrothermal reaction kettle at 110-300 degrees C, reacting for 1-100 hours, filtering, washing and drying the product, obtaining chromium hydroxide hydrate nanosheet, calcining obtained chromium hydroxide hydrate oxide nanosheet under the protection of argon gas or other inert gas at 200-1000 degrees C for 0.1-10 hours.