▎ 摘 要
NOVELTY - Treating waste liquid produced during preparation of graphene oxide comprises adding neutralizing agent to waste liquid; when the pH is raised to 5-8, adding precipitating agent; where the neutralizing agent is basic compound containing nitrogen; and precipitating agent is compound containing oxalate (C2O4(2-)). USE - The method is useful for treating waste liquid produced during preparation of graphene oxide. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: (1) environmentally-friendly preparing graphene oxide comprises preparing graphene oxide by graphite oxide reduction method, and treating produced waste liquid by above mentioned method; and (2) environmentally-friendly preparing graphene comprising (1) preparing graphene oxide by above mentioned, and (2) subjecting the graphene oxide obtained in the step (1) to chemical reduction or thermal reduction.