▎ 摘　　要

NOVELTY - Synthesizing an adsorption-photocatalytic composite based on UIO-66-NH2 and graphene in situ co-assembly comprises (i) taking grapheme, dissolving in the preparation of N,N-dimethylformamide, ultrasonically processing, (ii), adding 2-amino-acid ligand into solution A, ultrasonic process and stirring, (iii), taking the precursor used to synthesize MOF zirconium tetrachloride, dissolving into solution B ultrasonic process and stirring, (iv), adding the solution C in the microwave reacting, (v) taking the obtained composite material the product centrifuging and washing. USE - The method is useful for synthesizing an adsorption-photocatalytic composite based on UIO-66-NH2 and graphene in situ co-assembly (claimed). DETAILED DESCRIPTION - Synthesizing an adsorption-photocatalytic composite based on UIO-66-NH2 and graphene in situ co-assembly comprises (i) taking 0.5-3.0 % grapheme, dissolving in the preparation of N,N-dimethylformamide, ultrasonically processing, so that graphene is dissolved in the solution to obtain solution A, (ii), adding 2-amino-acid ligand into solution A, ultrasonic process and stirring to obtain the solution B, (iii), taking the precursor used to synthesize MOF zirconium tetrachloride, dissolving into solution B ultrasonic process and stirring to obtain solution C, where the mass ratio of the 2-amino-terephthalic acid ligand in step (ii) to the precursor zirconium tetrachloride in step (iii) is 1:1.3, (iv), adding the solution C in the microwave reacting for 1-60 minutes to obtain the product, (v) taking the obtained composite material the product centrifuging and washing.