• 专利标题:   Preparation of high-adhesiveness polyester hot-melt adhesive used for quick bonding of shoes, involves esterifying fatty acid, aliphatic diacid and diol, adding thermoplastic elastomer and graphene and polycondensing mixture.
  • 专利号:   CN106189983-A, CN106189983-B
  • 发明人:   MA A
  • 专利权人:   MA A, JIEYANG LIANGFENGDA METALS PLASTIC
  • 国际专利分类:   C08G063/685, C09J011/04, C09J011/06, C09J167/06, C09J175/04
  • 专利详细信息:   CN106189983-A 07 Dec 2016 C09J-167/06 201721 Pages: 5 Chinese
  • 申请详细信息:   CN106189983-A CN10595927 27 Jul 2016
  • 优先权号:   CN10595927

▎ 摘  要

NOVELTY - Long-chain fatty acid, medium-chain aliphatic diacid and branched-chain 8C or less diol are esterified (e1) at 180-210 degrees C in presence of antimony(III) acetate as catalyst under nitrogen protection until water content reaches theoretical amount (95% or more). Terephthalic acid, dimer acid, hexamethylenediamine, butanediol and glycerol are added to mixture and esterified (e2) at 180-220 degrees C. Thermoplastic elastomer, coupling agent, heat stabilizers and graphene are added to mixture and polycondensed for 0.5 hour under reduced pressure, to obtain high-adhesiveness polyester hot-melt adhesive. USE - Preparation of high-adhesiveness polyester hot-melt adhesive used for quick bonding of shoes (claimed). ADVANTAGE - The method enables preparation of polyester hot-melt adhesive has excellent adhesiveness.