• 专利标题:   Preparation of modified graphene reinforced flame retardant recycled polyester staple fiber involves taking paris rhizome, crushing, adding ethanol, extracting with combining extracts, concentrating, and adding petroleum ether.
  • 专利号:   CN105671677-A
  • 发明人:   LI J
  • 专利权人:   ZHANGJIAGANG ANSHUN SCI TECHNOLOGY DEV
  • 国际专利分类:   D01F001/07, D01F006/92
  • 专利详细信息:   CN105671677-A 15 Jun 2016 D01F-006/92 201666 Pages: 8 Chinese
  • 申请详细信息:   CN105671677-A CN10118416 02 Mar 2016
  • 优先权号:   CN10118416

▎ 摘  要

NOVELTY - A modified graphene reinforced flame retardant recycled polyester staple fiber is prepared by taking paris rhizome, crushing, adding 75-85 wt.% ethanol, extracting with combining extracts, concentrating, adding petroleum ether, ethyl acetate and saturated n-butanol, extracting respectively, taking ethyl acetate extract, purifying via macroporous resin, eluting with 50 wt.% ethanol, collecting eluate, concentrating, separating via normal phase silica gel and octadecyl silane bonded silica reversed-phase separation, eluting with 75 wt.% methanol aqueous solution, and collecting eluent. USE - Method for preparing modified graphene reinforced flame retardant recycled polyester staple fiber (claimed). ADVANTAGE - The fiber has increased far infrared fiber mechanical property and strength. DETAILED DESCRIPTION - A modified graphene reinforced flame retardant recycled polyester staple fiber is prepared by taking paris rhizome, crushing, adding 75-85 wt.% ethanol, extracting with combining extracts, concentrating, adding petroleum ether, ethyl acetate and saturated n-butanol, extracting respectively, taking ethyl acetate extract, purifying via macroporous resin, eluting with 50 wt.% ethanol, collecting eluate, concentrating, separating via normal phase silica gel and octadecyl silane bonded silica reversed-phase separation, eluting with 75 wt.% methanol aqueous solution, collecting eluent, concentrating, adding graphene solution and surfactant, stirring at 15-80 degrees C for 30-120 minutes, mixing, ultrasonicating, removing solvent, adding fiber masterbatch, mixing, drying at 90-140 degrees C, homogenizing for 10-25 minutes, filtering, melt spinning at 275-278 degrees C, drafting, cutting, and packing.