• 专利标题:   Preparing a graphene type molybdenum disulfide material comprises e.g. mixing molybdenite and intercalating agent, adding organic solvent to form a mixed turbid liquid, introducing the mixed turbid liquid into grinding mill and grinding.
  • 专利号:   CN107758746-A
  • 发明人:   SUN W, JI X, JIANG F, HOU H, TANG H, LI S, ZHAO W
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   C01G039/06
  • 专利详细信息:   CN107758746-A 06 Mar 2018 C01G-039/06 201824 Pages: 10 Chinese
  • 申请详细信息:   CN107758746-A CN11169336 22 Nov 2017
  • 优先权号:   CN11169336

▎ 摘  要

NOVELTY - Preparing a graphene type molybdenum disulfide material comprises (i) mixing molybdenite and intercalating agent and adding organic solvent to form a mixed turbid liquid, (ii) introducing the mixed turbid liquid into the grinding mill from the feed inlet,, grinding for greater than or equal to 12 hours, obtaining the material from the discharge port, providing the mill with a bearing and a sleeve, filling the cylinder sleeve and the bearing with rod-type medium and (iii) crushing the milled material by an ultrasonic crusher, separating the solid particles to obtain solid particles and drying. USE - The method is useful for preparing a graphene type molybdenum disulfide material. ADVANTAGE - The method is simple and stable. The material has good performance. DETAILED DESCRIPTION - Preparing a graphene type molybdenum disulfide material comprises (i) mixing molybdenite and ntercalating agent and adding organic solvent to form a mixed turbid liquid, where the mass fraction of the molybdenum disulfide in the mixed turbid liquid is 5-25%, (ii) introducing the mixed turbid liquid into the grinding mill from the feed inlet, grinding for greater than or equal to 12 hours, obtaining the material from the discharge port, providing the mill with a bearing and a sleeve, filling the cylinder sleeve and the bearing with rod-type medium, where the filling rate of the rod medium in the mill cavity is 80-97% and (iii) crushing the milled material by an ultrasonic crusher, where the frequency of the ultrasonic wave is 40-100 KHZ, separating the solid particles to obtain solid particles and drying.