• 专利标题:   Preparing maleic anhydride-modified graphene oxide/bismaleimide nano-composite material used in e.g. automobiles, by mixing graphene oxide, maleic anhydride, 2,2'-diallyl bisphenol-A and 4,4'-diphenylmethane bismaleimide and curing.
  • 专利号:   CN105218815-A, CN105218815-B
  • 发明人:   LI W, LU S, MA K, REN R, WANG B, WANG M, YUE Y
  • 专利权人:   UNIV SHENYANG AEROSPACE
  • 国际专利分类:   C08G073/12, C08K003/04, C08K009/02, C08K009/04
  • 专利详细信息:   CN105218815-A 06 Jan 2016 C08G-073/12 201643 Pages: 6 English
  • 申请详细信息:   CN105218815-A CN10583578 15 Sep 2015
  • 优先权号:   CN10583578

▎ 摘  要

NOVELTY - Preparation of maleic anhydride-modified graphene oxide/bismaleimide nano-composite material involves mixing graphene oxide and solvent, ultrasonically-dispersing, adding graphene oxide and maleic anhydride, reacting, cooling, washing with ethanol to remove unreacted maleic anhydride, drying, lyophilizing to obtain maleic anhydride-modified graphene oxide, adding 2,2- diallyl bisphenol-A, ultrasonically-dispersing, adding 4,4'-diphenylmethane bismaleimide and prepolymer resin, preheating, molding, placing, curing and cooling. USE - Preparation of maleic anhydride-modified graphene oxide/bismaleimide nano-composite material useful in aerospace applications, automobiles, shipbuilding, machinery and electronics. DETAILED DESCRIPTION - Preparation of maleic anhydride-modified graphene oxide/bismaleimide nano-composite material involves mixing graphene oxide and solvent, ultrasonically-dispersing at power of 100-1000 Watts and frequency of 15-40 Hz, adding graphene oxide in a mass ratio of 1:1-500, adding maleic anhydride, reacting for 0.5-3 hours, cooling to room temperature, washing with ethanol to remove unreacted maleic anhydride, drying and then lyophilizing to obtain maleic anhydride-modified graphene oxide, adding 2,2- diallyl bisphenol-A, ultrasonically-dispersing at power of 100-1000 Watts and frequency of 15-40 Hz for 1-1.5 hours, adding 4,4'-diphenylmethane bismaleimide and prepolymer resin, preheating, molding, placing in an oven at 60-130 degrees C, curing at 140 degrees C for 1 hour and cooling.