• 专利标题:   Preparing graphene molybdenum disulfide-graphene composite material, involves adding molybdenum disulfide powder to intercalation solution, and adding potassium chlorate, sodium nitrate, sulfuric acid and hydrogen peroxide.
  • 专利号:   CN106622297-A, CN106622297-B
  • 发明人:   HU P, WANG K, CHEN Z, CHANG T, DENG J, YANG F, HU B, LI Q, ZHOU Y, GAO Y
  • 专利权人:   UNIV XIAN ARCHITECTURE TECHNOLOGY, UNIV XIAN ARCHITECTURE TECHNOLOGY
  • 国际专利分类:   B01J027/051, B01J035/00
  • 专利详细信息:   CN106622297-A 10 May 2017 B01J-027/051 201740 Pages: 17 Chinese
  • 申请详细信息:   CN106622297-A CN10962902 04 Nov 2016
  • 优先权号:   CN10962902

▎ 摘  要

NOVELTY - The method for preparing graphene molybdenum disulfide-graphene composite material, involves adding molybdenum disulfide powder to intercalation solution, drying to obtain intercalated molybdenum disulfide powder, reacting molybdenum disulfide powder with potassium chlorate, sodium nitrate, 98% concentration of sulfuric acid and 30% concentration of hydrogen peroxide, mixing intercalated molybdenum disulfide powder and protein substances with water, drying, grinding to obtain precursor powder, carrying out reduction reaction and grinding to obtain final product. USE - Method for preparing graphene molybdenum disulfide-graphene composite material (claimed). ADVANTAGE - The method enables preparation of graphene molybdenum disulfide-graphene composite material by one-step process. DETAILED DESCRIPTION - Method for preparing graphene molybdenum disulfide-graphene composite material, involves (1) adding molybdenum disulfide powder to intercalation solution for intercalation reaction, drying to obtain intercalated molybdenum disulfide powder, reacting molybdenum disulfide powder with potassium chlorate, sodium nitrate, 98% concentration of sulfuric acid and 30% concentration of hydrogen peroxide in a ratio of 1 g:(1-4) g:(0.5-2) g:(9-40) mL:(4-20) mL, (2) mixing intercalated molybdenum disulfide powder and protein substances with water, stirring evenly, drying, grinding to obtain precursor powder, (3) carrying out reduction reaction of precursor powder under protective gas, removing the reaction product and grinding to obtain graphene molybdenum disulfide-graphene composite material. The intercalation solution is selected from potassium chlorate, sodium nitrate, concentrated sulfuric acid and hydrogen peroxide. The ratio of intercalated molybdenum disulfide powder, protein and water is 2 g:(2-7) g:(20-70) g.